Pergamon Series in Analytical Chemistry, Volume 2: Basic Analytical Chemistry brings together numerous studies of the vast expansion in the use of classical and instrumental methods of analysis. This book is composed of six chapters. After providing a theoretical background of analytical chemistry, this book goes on dealing with the fundamental principles of chemical equilibria in solution. The subsequent chapters consider the advances in qualitative and quantitative chemical analyses. These chapters present a unified view of these analyses based on the Bronsted-Lowry theory and the donor-acceptor principle. These topics are followed by discussions on instrumental analysis using various methods, including electrochemical, optical, spectroscopic, and thermal methods, as well as radioactive isotopes. The finals chapters examine the separation methods and the essential features of organic chemical analysis that are different from methods for inorganic compounds. This book is of value to analytical chemists and researchers.
Author: L. Pataki,E. Zapp
Analytical Chemistry Has Made Significant Progress In The Last Two Decades. Several Methods Have Come To The Forefront While Some Classical Methods Have Been Relegated. An Attempt Has Been Made In This Edition To Strike A Balance Between These Two Extremes, By Retaining Most Significant Methods And Incorporating Some Novel Techniques. Thus An Endeavour Has Been Made To Make This Book Up To Date With Recent Methods.The First Part Of This Book Covers The Classical Volumetric As Well As Gravimetric Methods Of Analysis. The Separation Methods Are Prerequisite For Dependable Quantitative Methods Of Analysis. Therefore Not Only Solvent Extraction Separations But Also Chromatographic Methods Such As Adsorption, Partition, Ion- Exchange, Exclusion Andelectro Chromatography Have Been Included. To Keep Pace With Modern Developments The Newly Discovered Techniques Such As Ion Chromatography, Super-Critical Fluid Chromatography And Capillary Electrophoresis Have Been Included.The Next Part Of The Book Encompases The Well Known Spectroscopic Methods Such As Uv, Visible, Ir, Nmr, And Esr Techniques And Also Atomic Absorption And Plasma Spectroscopy And Molecular Luminescences Methods. Novel Analytical Techniques Such As Auger, Esca And Photo Accoustic Spectroscopy Of Surfaces Are Also Included.The Final Part Of This Book Covers Thermal And Radioanalytical Methods Of Analysis. The Concluding Chapters On Electroanalytical Techniques Include Potientometry, Conductometry. Coulometry And Voltametry Inclusive Of All Kinds Of A Polarography. The Theme Of On Line Analysis Is Covered In Automated Methods Of Analysis.To Sustain The Interest Of The Reader Each Chapter Is Provided With Latest References To The Monographs In The Field. Further, To Test The Comprehension Of The Subject Each Chapter Is Provided With Large Number Of Solved And Unsolved Problems.This Book Should Be Useful To Those Reads Who Have Requisite Knowledge In Chemistry And Are Majoring In Analytical Chemistry. It Is Also Useful To Practising Chemists Whose Sole Aim Is To Keep Abreast With Modern Developments In The Field.
Author: S M Khopkar
Publisher: New Age International
BASIC ANALYTICAL CHEMISTRY Malaysia is a fast developing country. Realizing the need to provide experts in chemistry,this book is appropriate to be used as a text for fundamental course in analytical chemistry. The texts cover topics from the most basic analytical chemistry course including methods on basic analyses to important concepts such as handling of data analysis, chemical equilibrium, stoichiometry and titration. The chemical equilibrium in this book covers acid-base equilibrium, precipitation, complex and redox titration. For every topic, examples and solutions are provided to give reader a better understanding in the topics covered.
Author: Faiz Bukhari Mohd Suah,Wan Saime Wan Ngah,Che Sofiah Saidin
Publisher: Penerbit USM
Principles of Analytical Chemistry gives readers a taste of what the field is all about. Using keywords of modern analytical chemistry, it constructs an overview of the discipline, accessible to readers pursuing different scientific and technical studies. In addition to the extremely easy-to-understand presentation, practical exercises, questions, and lessons expound a large number of examples.
Author: Miguel Valcarcel
Publisher: Springer Science & Business Media
This book offers a completely new approach to learning and teaching the fundamentals of analytical chemistry. It summarizes 250 basic concepts of the field on the basis of slides. Each of the nine chapters offers the following features: • Introduction: Summary. General scheme. Teaching objectives. • Text containing the explanation of each slide. • Recommended and commented bibliography. • Questions to be answered. • Slides. A distinct feature of this novel book is its focus on the fundamental concepts and essential principles of analytical chemistry, which sets it apart from other books presenting descriptive overviews of methods and techniques.
A Teaching–Learning Approach
Author: Miguel Valcárcel Cases,Ángela I. López-Lorente,Ma Ángeles López-Jiménez
This book is an introductory manual that explains the basic concepts of chemistry behind scientific analytical techniques and that reviews their application to archaeology. It explains key terminology, outlines the procedures to be followed in order to produce good data, and describes the function of the basic instrumentation required to carry out those procedures. The manual contains chapters on the basic chemistry and physics necessary to understand the techniques used in analytical chemistry, with more detailed chapters on Atomic Absorption, Inductively Coupled Plasma Emission Spectroscopy, Neutron Activation Analysis, X-ray Flourescence, Electron Microscopy, Infra-red and Raman Spectroscopy, and Mass Spectrometry. Each chapter describes the operation of the instruments, some hints on the practicalities, and a review of the application of the technique to archaeology, including some case studies. With guides to further reading on the topic, it is an essential tool for practitioners, researchers and advanced students alike.
Author: A. M. Pollard
Publisher: Cambridge University Press
Proteomic Profiling and Analytical Chemistry helps scientists without a strong background in analytical chemistry to understand basic analytical principles and apply them to proteomics profiling. In most proteomic profiling experiments, liquid chromatography is used; this method is also used widely in analytical chemistry. This book bridges the gap between overly specialized courses and books in mass spectrometry, proteomics and analytical chemistry. It also helps researchers with an analytical chemistry background to break into the proteomics field. Proteomic Profiling and Analytical Chemistry focuses on practical applications for proteomic research helping readers to design better experiments and to more easily interpret, analyze and validate the resulting data. Experimental aspects such as sample preparation, protein extraction and precipitation, gel electrophoresis, microarrays, dynamics of fluorescent dyes, and more are all covered in detail. Covers the analytical consequences of protein and peptide modifications that may have a profound effect on how and what researchers actually measure Includes practical examples illustrating the importance of problems in quantitation and validation of biomarkers Helps in designing and executing proteomic experiments with sound analytics
Author: Pawel Ciborowski,Jerzy Silberring
Table of Contents - Chapter 1. Analytical Objectives, or - What Analytical Chemists Do; Chapter 2. Basic Tools and Operations of Analytical Chemistry; Chapter 3. Data Handling and Spreadsheets in Analytical Chemistry; Chapter 4. Good Laboratory Practice; Quality Assurance; Chapter 5. Stoichiometric Calculations; The Workhorse of the Analyst; Chapter 6. General Concepts of Chemical Equilibrium; Chapter 7.Acid Base Equilibria; Chapter 8, Acid Base Titrations; Chapter 9. Complexometric Reactions and Titrations; Chapter 10. Gravimetric Analysis and Precipitation Equilibria; Chapter 11. Precipitation Reactions and Titrations; Chapter 12. Electrochemical Cells and Electrode Potentials; Chapter 13. Potentiometric Electrodes and Potentiometry;Chapter 14. Redox and Potentiometric Titrations; Chapter 15. Voltammetry and Electrochemical Sensors; Chapter 16. Spectro Chemical Methods; Chapter 17. Atomic Spectrometric Methods; Chapter 18.Sample Preparation; Solvent and Solid-Phase Extraction; Chapter 19. Chromatography; Principles and Theory; Chapter 20. Gas Chromatography; Chapter 21. Liquid Chromatography; Chapter 22, Kinetic Methods of Analysis; Chapter 24. Clinical Chemistry; Chapter 25. Century of the Gene-Genomics and Proteomics; Dna Sequencing and Protein Profiling; Chapter 26. Environmental Sampling and Analysis; Experiments; Appendix A. Literature of Analytical Chemistry; Appendix B. Review of Mathematical Operations Exponents, Logarithms, the Quadratic Formula, and Calculators; Apendix C. Tables of Constants; Appendix D. Safety in the Laboratory; Appendix E. Periodic Tables on the Web; Appendix F. Answers to Some Even-Numbered Problems; Index.
Author: Gary D. Christian
Publisher: John Wiley & Sons Inc
Author: Ferenc Szabadváry
Category: Chemistry, Analytic
This new edition of a successful, bestselling book continues toprovide you with practical information on the use of statisticalmethods for solving real-world problems in complex industrialenvironments. Complete with examples from the chemical andpharmaceutical laboratory and manufacturing areas, this thoroughlyupdated book clearly demonstrates how to obtain reliable results bychoosing the most appropriate experimental design and dataevaluation methods. Unlike other books on the subject, Statistical Methods inAnalytical Chemistry, Second Edition presents and solves problemsin the context of a comprehensive decision-making process under GMPrules: Would you recommend the destruction of a $100,000 batch ofproduct if one of four repeat determinations barely fails thespecification limit? How would you prevent this from happening inthe first place? Are you sure the calculator you are using istelling the truth? To help you control these situations, the newedition: * Covers univariate, bivariate, and multivariate data * Features case studies from the pharmaceutical and chemicalindustries demonstrating typical problems analysts encounter andthe techniques used to solve them * Offers information on ancillary techniques, including a shortintroduction to optimization, exploratory data analysis, smoothingand computer simulation, and recapitulation of errorpropagation * Boasts numerous Excel files and compiled Visual Basic programs-nostatistical table lookups required! * Uses Monte Carlo simulation to illustrate the variabilityinherent in statistically indistinguishable data sets Statistical Methods in Analytical Chemistry, Second Edition is anexcellent, one-of-a-kind resource for laboratory scientists andengineers and project managers who need to assess data reliability;QC staff, regulators, and customers who want to frame realisticrequirements and specifications; as well as educators looking forreal-life experiments and advanced students in chemistry andpharmaceutical science. From the reviews of Statistical Methods in Analytical Chemistry,First Edition: "This book is extremely valuable. The authors supply many veryuseful programs along with their source code. Thus, the user cancheck the authenticity of the result and gain a greaterunderstanding of the algorithm from the code. It should be on thebookshelf of every analytical chemist."-Applied Spectroscopy "The authors have compiled an interesting collection of data toillustrate the application of statistical methods . . . includingcalibrating, setting detection limits, analyzing ANOVA data,analyzing stability data, and determining the influence of errorpropagation."-Clinical Chemistry "The examples are taken from a chemical/pharmaceutical environment,but serve as convenient vehicles for the discussion of when to usewhich test, and how to make sense out of the results. Whilepractical use of statistics is the major concern, it is put intoperspective, and the reader is urged to use plausibilitychecks."-Journal of Chemical Education "The discussion of univariate statistical tests is one of the morethorough I have seen in this type of book . . . The treatment oflinear regression is also thorough, and a complete set of equationsfor uncertainty in the results is presented . . . The bibliographyis extensive and will serve as a valuable resource for thoseseeking more information on virtually any topic covered in thebook."-Journal of American Chemical Society "This book treats the application of statistics to analyticalchemistry in a very practical manner. [It] integrates PC computingpower, testing programs, and analytical know-how in the context ofgood manufacturing practice/good laboratory practice (GMP/GLP) . ..The book is of value in many fields of analytical chemistry andshould be available in all relevant libraries."-Chemometrics andIntelligent Laboratory Systems
Author: Peter C. Meier,Richard E. Zünd
Publisher: John Wiley & Sons
The issue of quality assurance in the analytical chemistry laboratory has become of great importance in recent years. Quality in the Analytical Chemistry Laboratory introduces the reader to the whole concept of quality assurance. It discusses how all aspects of chemical analysis, from sampling and method selection to choice of equipment and the taking and reporting of measurements affect the quality of analytical data. Finally, the implementation and use of Quality Systems are covered. Quality in the Analytical Chemistry Laboratory is an indispensable volume for all those working in analytical chemistry laboratories, for all students of chemistry, whether specialising in analytical chemistry or not, and for laboratory managers wishing to introduce quality assurance methods into their laboratories. It is written by a team of members of staff at the Laboratory of the Government Chemist, each of whom has experience of working to international quality standards. Analytical Chemistry by Open Learning This series provides a uniquely comprehensive and integrated coverage of analytical chemistry, covering basic concepts, classical methods, instrumental techniques and applications. The learning objectives of each text are clearly identified and the student’s understanding of the material is constantly challenged by self-assessment questions with reinforcing or remedial responses. The overall objective of Analytical Chemistry by Open Learning is to enable the student to select and apply appropriate methods and techniques to solve analytical problems, and to interpret the results obtained.
Author: Elizabeth Prichard,Neil T. Crosby,Florence Elizabeth Prichard
Publisher: John Wiley & Sons
Quality Assurance in Chemical Measurement, an advanced EURACHEM textbook, provides in-depth but easy-to-understand coverage for training, teaching and continuing studies. The CD-ROM accompanying the book contains course materials produced by ten experienced specialists, including more than 750 overheads (graphics and text) in ready-to-use PowerPoint® documents in English and German language. The book will serve as an advanced textbook for analytical chemistry students and professionals in industry and service labs and as a reference text and source of course materials for lecturers. The second edition has been completely revised according to the newest legislation.
Training and Teaching
Author: Bernd W. Wenclawiak,Michael Koch,Evsevios Hadjicostas
Book envelops various analytical procedures including their principle and application in chemical and drug analysis.
Author: Deepak Chowrasia,Nisha Sharma
Publisher: Deepak Chowrasia
This thoroughly updated second edition of the ACOL text on Mass Spectrometry gives a modern approach to those beginning to use or study mass spectrometry. Self assessment questions and solutions are included. Fundamentals and modern instrumental techniques are also covered in this book.
Analytical Chemistry by Open Learning
Author: James Barker,David J. Ando,Reg Davis,Martin J. Frearson
Publisher: John Wiley & Sons
The complex field of analytical chemistry requires knowledge and application of the fundamental principles of numerical calculation. Problems of Instrumental Analytical Chemistry provides support and guidance to help students develop these numerical strategies to generate information from experimental results in an efficient and reliable way. Exercises are provided to give standard protocols to follow which address the most common calculations needed in the daily work of a laboratory. Also included are easy to follow diagrams to facilitate understanding and avoid common errors, making it perfect as a hands-on accompaniment to in-class learning. Subjects covered follow a course in analytical chemistry from the initial basics of data analysis, to applications of mass, UV-Vis, infrared and atomic spectrometry, chromatography, and finally concludes with an overview of nuclear magnetic resonance. Intended as a self-training tool for undergraduates in chemistry, analytic chemistry and related subjects, this book is also useful as a reference for scientists looking to brush up on their knowledge of instrumental techniques in laboratories. Request Inspection Copy
A Hands-On Guide
Author: JM Andrade-Garda,A Carlosena-Zubieta,MP GÃ³mez-Carracedo,MA Maestro-Saavedra,MC Prieto-Blanco,RM Soto-Ferreiro
Publisher: World Scientific Publishing Company
The third edition of this long-selling introductory textbook and ready reference covers all pertinent topics, from basic statistics via modeling and databases right up to the latest regulatory issues. The experienced and internationally recognized author, Matthias Otto, introduces the statistical-mathematical evaluation of chemical measurements, especially analytical ones, going on to provide a modern approach to signal processing, designing and optimizing experiments, pattern recognition and classification, as well as modeling simple and nonlinear relationships. Analytical databases are equally covered as are applications of multiway analysis, artificial intelligence, fuzzy theory, neural networks, and genetic algorithms. The new edition has 10% new content to cover such recent developments as orthogonal signal correction and new data exchange formats, tree based classification and regression, independent component analysis, ensemble methods and neuro-fuzzy systems. It still retains, however, the proven features from previous editions: worked examples, questions and problems, additional information and brief explanations in the margin.
Statistics and Computer Application in Analytical Chemistry
Author: Matthias Otto
Publisher: John Wiley & Sons
Interdisciplinary knowledge is becoming more and more important to the modern scientist. This invaluable textbook covers bioanalytical chemistry (mainly the analysis of proteins and DNA) and explains everything for the nonbiologist. Electrophoresis, mass spectrometry, biosensors, bioassays, DNA and protein sequencing are not necessarily all included in conventional analytical chemistry textbooks. The book describes the basic principles and the applications of instrumental and molecular methods. It is particularly useful to chemistry and engineering students who already have some basic knowledge about analytical chemistry.
Author: Andreas Manz,Nicole Pamme,Dimitri Iossifidis
Publisher: Imperial College Press